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Building an electrode (each group should build 2)

  • Cut a piece of nickel mesh to cover the flange of the syringe cylinder completely
  • Place an aluminum plate on a heating plate. Place the baking paper on the Al plate and the nickel net on the paper.
  • Heat the plate to a temperature that will melt the plastic but not burn it.
  • 4. Place the flange of the syringe on the nickel net on the heating plate. Press down firmly so that the nickel net is melted onto the flange. Make sure that the net is sealed tight to the whole of the flange surface, but take care not to melt so much plastic that the cylinder hold itself is covered with molten plastic.
  • Remove the syringe and net form the eating plate and allow to cool.
  • At one of the sides of the flange drill a hole through the flange using the electric drill. Place a piece of wood beneath to prevent drilling into the lab bench. (see picture) Push the machine screw through the hole and fasten using a washer and nut. (see picture)
  • Mount a piece of insulated copper wire around the machine screw by twisting an end into a loop with a flat bit and fastening it with the nut. Tighten it so that good electrical contact is established between the wire and the nickel net. Use tape to attach the wire to the syringe cylinder.
  • Cut off excess nickel net around the flange.
  • Clean the nickel net by immersing the electrode in 4M nitric acid for at least five minutes. Also clean the extra piece of nickel net in this manner. This much be carried out in the fume hood since poisonous flumes may evolve. Rinse thoroughly with water.
  • Place the nickel net of the electrode in a solution of palladium chloride for 30 minutes and then gently rinse with water. Be sure to put the extra piece of nickel net in the palladium chloride solution as well. The electrode is now ready. You should have something that resembles the picture.

Figure 1: Drilling holes in flange.

Figure 2: Wire connection assembly.

Figure 3: Final assembled cell

Building the cell

  • First cut top off of one of the syringes. This will be the electrode you introduce the liquid/solid fuel.
  • Place your two electrodes into a 600mL beaker containing 1M NaOH solution. The nickel meshing should be completely submerged in solution.
  • Fill a balloon with oxygen gas (from gas cylinder) and connect using rubber hosing to the syringe that was not cut. The oxygen may bubble slowly through the syringe.
  • Roll up the extra piece of nickel mesh and place into the cut syringe.
  • Add ~20mg of NaBH4 to the syringe with the extra piece of nickel mesh. If time permits you may test other fuels later.

Figure 4: Functional cell layout.

Testing the cell

  • Measure the voltage generated by your cell by taking a digital multimeter and setting it to DC voltage. Connect one probe to each wire of the cell. The reading may continue to grow for a while and then stabilize. Record this stable voltage. It should read between 0.8V-1V.
  • Measure the current your cell sources by keeping the probes connected and switching to current mode. This reading should be between 30mA-50mA.

Questions & Answers

how does Neisseria cause meningitis
Nyibol Reply
what is microbiologist
Muhammad Reply
what is errata
Muhammad
is the branch of biology that deals with the study of microorganisms.
Ntefuni Reply
What is microbiology
Mercy Reply
studies of microbes
Louisiaste
when we takee the specimen which lumbar,spin,
Ziyad Reply
How bacteria create energy to survive?
Muhamad Reply
Bacteria doesn't produce energy they are dependent upon their substrate in case of lack of nutrients they are able to make spores which helps them to sustain in harsh environments
_Adnan
But not all bacteria make spores, l mean Eukaryotic cells have Mitochondria which acts as powerhouse for them, since bacteria don't have it, what is the substitution for it?
Muhamad
they make spores
Louisiaste
what is sporadic nd endemic, epidemic
Aminu Reply
the significance of food webs for disease transmission
Abreham
food webs brings about an infection as an individual depends on number of diseased foods or carriers dully.
Mark
explain assimilatory nitrate reduction
Esinniobiwa Reply
Assimilatory nitrate reduction is a process that occurs in some microorganisms, such as bacteria and archaea, in which nitrate (NO3-) is reduced to nitrite (NO2-), and then further reduced to ammonia (NH3).
Elkana
This process is called assimilatory nitrate reduction because the nitrogen that is produced is incorporated in the cells of microorganisms where it can be used in the synthesis of amino acids and other nitrogen products
Elkana
Examples of thermophilic organisms
Shu Reply
Give Examples of thermophilic organisms
Shu
advantages of normal Flora to the host
Micheal Reply
Prevent foreign microbes to the host
Abubakar
they provide healthier benefits to their hosts
ayesha
They are friends to host only when Host immune system is strong and become enemies when the host immune system is weakened . very bad relationship!
Mark
what is cell
faisal Reply
cell is the smallest unit of life
Fauziya
cell is the smallest unit of life
Akanni
ok
Innocent
cell is the structural and functional unit of life
Hasan
is the fundamental units of Life
Musa
what are emergency diseases
Micheal Reply
There are nothing like emergency disease but there are some common medical emergency which can occur simultaneously like Bleeding,heart attack,Breathing difficulties,severe pain heart stock.Hope you will get my point .Have a nice day ❣️
_Adnan
define infection ,prevention and control
Innocent
I think infection prevention and control is the avoidance of all things we do that gives out break of infections and promotion of health practices that promote life
Lubega
Heyy Lubega hussein where are u from?
_Adnan
en français
Adama
which site have a normal flora
ESTHER Reply
Many sites of the body have it Skin Nasal cavity Oral cavity Gastro intestinal tract
Safaa
skin
Asiina
skin,Oral,Nasal,GIt
Sadik
How can Commensal can Bacteria change into pathogen?
Sadik
How can Commensal Bacteria change into pathogen?
Sadik
all
Tesfaye
by fussion
Asiina
what are the advantages of normal Flora to the host
Micheal
what are the ways of control and prevention of nosocomial infection in the hospital
Micheal
what is inflammation
Shelly Reply
part of a tissue or an organ being wounded or bruised.
Wilfred
what term is used to name and classify microorganisms?
Micheal Reply
Binomial nomenclature
adeolu
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Source:  OpenStax, Honors chemistry lab fall. OpenStax CNX. Nov 15, 2007 Download for free at http://cnx.org/content/col10456/1.16
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