<< Chapter < Page Chapter >> Page >

High energy beam electrons are elastic scattered back from the surface. This type of signal gives information about chemical composition of the surface because the energy of backscattered electrons depends on the weight of atoms within the interaction layer. Also this type of electrons can form secondary electrons and escape from the surface or travel father into the sample than the secondary. The SEM image formed is the result of the intensity of the secondary electron emission from the sample at each x,y data point during the scanning of the surface.

Atomic force microscopy

AFM is a very popular tool to study surface dissolution. AFM set up consists of scanning a sharp tip on the end of a flexible cantilever which moves across a sample surface. The tips typically have an end radius of 2 to 20 nm, depending on tip type. When the tip touch the surface the forces of these interactions leads to deflection of a cantilever. The interaction between tip and sample surface involve mechanical contact forces, van der Waals forces, capillary forces, chemical bonding, electrostatic forces, magnetic forces etc. The deflection of a cantilever is usually measured by reflecting a laser beam off the back of the cantilever into a split photodiode detector. A schematic drawing of AFM can be seen in [link] . The two most commonly used modes of operation are contact mode AFM and tapping mode AFM, which are conducted in air or liquid environments.

Schematic drawing of an AFM apparatus.

Working under the contact mode AFM scans the sample while monitoring the change in cantilever deflection with the split photodiode detector. Loop maintains a constant cantilever reflection by vertically moving the scanner to get a constant signal. The distance which the scanner goes by moving vertically at each x,y data point is stored by the computer to form the topographic image of the sample surface. Working under the tapping mode AFM oscillates the cantilever at its resonance frequency (typically~300 kHz) and lightly “taps” the tip on the surface during scanning. The electrostatic forces increase when tip gets close to the sample surface, therefore the amplitude of the oscillation decreases. The laser deflection method is used to detect the amplitude of cantilever oscillation. Similar to the contact mode, feedback loop maintains a constant oscillation amplitude by moving the scanner vertically at every x,y data point. Recording this movement forms the topographical image. The advantage of tapping mode over contact mode is that it eliminates the lateral, shear forces present in contact mode. This enables tapping mode to image soft, fragile, and adhesive surfaces without damaging them while work under contact mode allows the damage to occur.

Comparison of techniques

All techniques described above are widely used in studying of surface nano- and micromorphology. However, each method has its own limitations and the proper choice of analytical technique depends on features of analyzed surface and primary goals of research.

Questions & Answers

Do somebody tell me a best nano engineering book for beginners?
s. Reply
what is fullerene does it is used to make bukky balls
Devang Reply
are you nano engineer ?
what is the Synthesis, properties,and applications of carbon nano chemistry
Abhijith Reply
so some one know about replacing silicon atom with phosphorous in semiconductors device?
s. Reply
Yeah, it is a pain to say the least. You basically have to heat the substarte up to around 1000 degrees celcius then pass phosphene gas over top of it, which is explosive and toxic by the way, under very low pressure.
how to fabricate graphene ink ?
for screen printed electrodes ?
What is lattice structure?
s. Reply
of graphene you mean?
or in general
in general
Graphene has a hexagonal structure
On having this app for quite a bit time, Haven't realised there's a chat room in it.
what is biological synthesis of nanoparticles
Sanket Reply
what's the easiest and fastest way to the synthesize AgNP?
Damian Reply
types of nano material
abeetha Reply
I start with an easy one. carbon nanotubes woven into a long filament like a string
many many of nanotubes
what is the k.e before it land
what is the function of carbon nanotubes?
I'm interested in nanotube
what is nanomaterials​ and their applications of sensors.
Ramkumar Reply
what is nano technology
Sravani Reply
what is system testing?
preparation of nanomaterial
Victor Reply
Yes, Nanotechnology has a very fast field of applications and their is always something new to do with it...
Himanshu Reply
good afternoon madam
what is system testing
what is the application of nanotechnology?
In this morden time nanotechnology used in many field . 1-Electronics-manufacturad IC ,RAM,MRAM,solar panel etc 2-Helth and Medical-Nanomedicine,Drug Dilivery for cancer treatment etc 3- Atomobile -MEMS, Coating on car etc. and may other field for details you can check at Google
anybody can imagine what will be happen after 100 years from now in nano tech world
after 100 year this will be not nanotechnology maybe this technology name will be change . maybe aftet 100 year . we work on electron lable practically about its properties and behaviour by the different instruments
name doesn't matter , whatever it will be change... I'm taking about effect on circumstances of the microscopic world
how hard could it be to apply nanotechnology against viral infections such HIV or Ebola?
silver nanoparticles could handle the job?
not now but maybe in future only AgNP maybe any other nanomaterials
I'm interested in Nanotube
this technology will not going on for the long time , so I'm thinking about femtotechnology 10^-15
can nanotechnology change the direction of the face of the world
Prasenjit Reply
At high concentrations (>0.01 M), the relation between absorptivity coefficient and absorbance is no longer linear. This is due to the electrostatic interactions between the quantum dots in close proximity. If the concentration of the solution is high, another effect that is seen is the scattering of light from the large number of quantum dots. This assumption only works at low concentrations of the analyte. Presence of stray light.
Ali Reply

Get the best Nanomaterials and nano... course in your pocket!

Source:  OpenStax, Nanomaterials and nanotechnology. OpenStax CNX. May 07, 2014 Download for free at http://legacy.cnx.org/content/col10700/1.13
Google Play and the Google Play logo are trademarks of Google Inc.

Notification Switch

Would you like to follow the 'Nanomaterials and nanotechnology' conversation and receive update notifications?